Series 4540 High Pressure Reactors, 600 & 1200 mL
This series of stirred reactors has been designed for users who need higher operating pressures than the 1900 to 2900 psi offered by the General Purpose Reactors, but do not require the high operating temperatures provided by the Series 4570 High Pressure, High Temperature Reactors. The 4540 series reactors offer working pressures to 5000 psi (345 bar) at temperatures to 350 °C.
These vessels have been designed with outside dimensions comparable to the Series 4520 and 4530 Reactors so that they can use the same support system, stirrer drive and heater as these popular general purpose models. This provides not only an attractively priced, high pressure/moderate temperature system, but also reactors that can be interchanged with the 1 and 2 liter sizes. The thicker walls required for higher operating pressures reduce the volumes of these reactors to 600 and 1200 mL.
These reactors can be used in either the bench top or floor stand mountings. While the 1200 mL reactor is offered as a fixed head bench top model; it is too tall and too heavy to be handled comfortably on a standard height bench top. It is recommended that the floor stand support option should be selected unless the user has an adjustable bench top which will accommodate the overall height of the 1200 mL systems.
Series 4540 Pressure Reactor System Specifications
Shaded bar indicates specifications that change within series.
Model Number – Moveable Vessel
4544
—
4544A
4544C
4546C
Model Number – Fixed Head
4545
4547
4545A
4547A
Approximate Volume, mL
600
1200
Maximum Pressure (MAWP)
5000 psi (345 bar)
Maximum Temperature
with PTFE Flat Gasket
350 °C
Reactor Details
Mounting Style
Moveable or Fixed Head
Stand Type
Bench Top
Floor Stand
Moveable Cart
Closure
Split-Ring (8 Compression Bolts for Flat Gasket,
no Compression Bolts for O-ring)
Valve Connections
1/4″ Male NPT
Magnetic Drive, Model No.
A1120HC6 General Purpose or A2140HC Footless
Maximum Torque
16 Inch-Pounds
Impeller(s), 6 blades
2 (1.75″ dia.)
Stirrer Motor
1/8 hp
1/4 hp
Pressure Gage, Size
4.5 inches
Range
0-5000 psi (345 bar)
Temperature Measurement
Thermowell
Cooling Coil (optional)
Serpentine or Loop
Bottom Drain Valve (BDV) (optional)
N/A
1″ NPS
Lift Mechanism
Pneumatic
Heater Style
Calrod
Heater Power, Watts
1000/1500
1500/2000
1300
Electrical Supply
Volts, AC
115 / 230
Maximum Load, amps, 115 / 230
12 / 9
Cylinder Dimensions
I.D. x Depth, inches
3.25 x 4.7
3.25 x 9.8
Vessel Assembly Weight, pounds
4544 : 50
4545 : 53
65
4544A : 50
4545A : 53
50
61
Cylinder Weight, pounds
18
29
Reactor/Stand Dimensions
Width x Depth, inches w/o Controller
17 x 24
21 x 28
35 x 18
Height, inches
38
48
63
Weight, pounds
125
135
175
185
Spare Parts Kit
4549M
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